Agilent TOF LC-MS 6230B
Serial Number: SG14090001
Sample Submission form
Submission form
SOPs
TOF Agilent ESI Source
General SOP
TOF Agilent APPI
Source
Manuals
TOF Agilent Intro
Manual
TOF Agilent
Maintenance Manual
Guidelines for choosing which ionization method to use
Procedure for removing amines
- remove HPLC column, do not run cleaning solution column
- make a 50/50 solution of IPA/water with 1% acetic acid, can go up to 10% acetic acid
- place nebulizer in a beaker
- run HPLC at 1 ml/min, DO NOT spray solution in mass spectrometer
- after rinse, flush with 50/50 ACN/Water and then reconnect nebulizer to mass spectrometer